The Mini-Kappa MK3 is a multi-axes goniometer head for MX crystallography beamlines.
It purveys additional κ & Φ axes, giving numerous possibilities of crystal reorientation. The Mini-kappa MK3 is a co-development of Arinax & the EMBL Grenoble Instrumentation Group (Cipriani team).
(κ) Kappa:
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Rotational precision: ±0.05°
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Travel Range: 0 to 255°
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Resolution: 0.35 mdeg
(ϕ) Phi:
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Rotational precision: ±0.09°
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Travel range: 360° (no limitation)
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Resolution: 1.41 mdeg
(Χ) Chi axis:
- Travel Range: 0 to 48°. Value depends of the kappa-axis’ position.
Easy & safe sample change
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Compatible with sample changer robot
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Adapted to vial or gripper based transfer
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Collision safe system
Fully-compatible with Arinax diffractometers
Available in standalone version
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Alone or with Arinax centering table
This video presents the Mini-Kappa Goniometer head mounted on a MD2-S microdiffractometer.
The Mini-Kappa is dedicated to MX crystallography synchrotron beamlines. It purveys additional Kappa & Phi axes, giving numerous possibilities of crystal reorientation.
The multi-axis goniometer head for MX crystallography
The Mini-Kappa MK3 is a multi-axis goniometer head with reduced dimensions that purveys additional κ & Φ axes, giving numerous possibilities of crystal reorientation.
It reaches a rotational precision of ±0.05° for κ axis & ±0.09° for Φ axis and can be equipped with the SmartMagnet sample holder.
Mounted on a MD3 High Precision X-ray diffractometer with an UP configuration, the Sphere of Confusion (SOC) that is achieved on the Ω axis is 100 nm.
Data Collection optimization
The mini-kappa MK3 considerably optimizes the data collection process by reducing the redundant protocol steps: it limits the number of diffractions needed to complete the data collection and avoids spot overlaps.
Sample Protection
Thanks to the additional kappa & Phi axes rotation, X-ray diffraction isn’t limited to one “crystal frame” but is realized on the entire crystal: the diffraction is more distributed over the crystal, limiting radiation damage.
Compact dimensions
Needed Volume that includes the Mini-kappa MK3 and the free space required for kappa movements is contained in a cylindrical volume with exceptional compact dimension of 120 mm length and 131 mm diameter.
Collision Safe System
The Mini-kappa MK3 is able to detect potential risk of collision with equipment, such as a robotic arm (e.g. Staubli robot). If an obstacle is on the path of the kappa movement, the integrated detector initiates the “Omega Stop” safety sequence: the kappa movement is stopped and information is conveyed to the beamline terminal.
Excellent compatibility
The Mini-kappa MK3 can be mounted on Arinax diffractometers, such as the MD3 & MD2-S x-ray microdiffractometers. The Mini-Kappa can also be compatible with other equipment.
Designed for modern MX crystallography beamlines, the Mini-kappa MK3 is compatible with sample changer robot using a vial or a gripper transfer, such as the 6-axis sample changer robots.
5 minutes Switchable Equipment
In order to give the best flexibility to users, the Mini-kappa MK3, the Plate manipulator and the SmartMagnet are designed to be easily mounted and dismounted according to user need: the switch from one to another takes about 5 minutes and only one person is required to do the switch.
Technical specifications
Sphere of Confusion | |
Measured on MD3-Up Ω axis | 100 nm radius @ 100 deg/s |
K Kappa axis | |
Angular range – Travel range – Resolution |
. 0 to 255° 0.35 mdeg |
Rotational precision | ±0.05° |
Φ Phi axis | |
Angular range – Travel range – Resolution |
. 360° (no limit) 1.41 mdeg |
Rotational precision | ±0.09° |
X Chi axis | |
Angular Range/Travel range | 0 to 48°. Kappa-axis position dependent. |
Sample pin requirement | |
International Standard “SPINE” | 22 mm length |
Motors | |
Stepper motors | |
Dimensions | |
Mini-kappa head (included needed volume for kappa movement) |
120 mm & 131 mm (L, D) |
Weight | |
280g |